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dc.contributor.authorRivera, Edisonpt_BR
dc.contributor.authorMuñoz Meneses, Rodrigo Arbeypt_BR
dc.contributor.authorMarín, Lorenapt_BR
dc.contributor.authorMora, Malkapt_BR
dc.contributor.authorTabares, Jesús A.pt_BR
dc.contributor.authorRodríguez, Luis A.pt_BR
dc.contributor.authorDiosa, Jesús E.pt_BR
dc.contributor.authorSivasamy, Rameshpt_BR
dc.contributor.authorMosquera Vargas, Edgarpt_BR
dc.date.accessioned2026-07-07T13:15:21Z-
dc.date.available2026-07-07T13:15:21Z-
dc.date.issued2025-12pt_BR
dc.identifier.citationRIVERA, Edison; MUÑOZ-MENESES, Rodrigo A.; MARÍN, Lorena; MORA, Malka; TABARES, Jesús A.; RODRÍGUEZ, Luis A.; DIOSA, Jesús E.; SIVASAMY, Ramesh; MOSQUERA-VARGAS, Edgar. Characterization of size- and shape-controlled magnetic iron oxide microspheres fabricated by the flame method from industrial steel waste. Emergent Materials, [S. l.], v. 8, n. 8, p. 7637-7649, 2025. DOI: https://doi.org/10.1007/s42247-025-01195-5. Disponível em: https://doi.org/10.1007/s42247-025-01195-5pt_BR
dc.identifier.urihttps://doi.org/10.1007/s42247-025-01195-5pt_BR
dc.identifier.urihttp://repositorio.unb.br/handle/10482/55279-
dc.language.isoeng-
dc.publisherSpringer Science and Business Media LLCpt_BR
dc.rightsAcesso Abertopt_BR
dc.titleCharacterization of size- and shape-controlled magnetic iron oxide microspheres fabricated by the flame method from industrial steel wastept_BR
dc.typeArtigopt_BR
dc.subject.keywordResíduos industriaispt_BR
dc.subject.keywordÓxidos de ferropt_BR
dc.subject.keywordMicropartículas esféricaspt_BR
dc.subject.keywordPropriedades magnéticaspt_BR
dc.rights.licenseOpen Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/.-
dc.identifier.doihttps://doi.org/10.1007/s42247-025-01195-5pt_BR
dc.description.abstract1Magnetic microspheres were fabricated from industrial waste via a single-stage flame spheroidization method using two ferric oxide precursor powders from steel hot rolling industry. The analysis of all samples was carried out by scanning electron microscopy (SEM), X-ray diffraction (XRD), Mössbauer spectroscopy, FTIR and Raman spectroscopy (RS), thermogravimetric analysis (TGA), and vibrating sample magnetometer (VSM). SEM, XRD, Mössbauer spectroscopy, FTIR and RS show the morphology, structure, and phases of the samples studied. The average size for each microsphere was 45 μm (Sample A2) and 60 μm (Sample B2). TGA confirmed the crystallization and phase transition of iron oxides. The VSM study showed high saturation magnetization (Ms ) for both microsphere samples, with the higher M s being very close to the reported value for bulk magnetite and exhibiting a very soft magnetic behavior. The flame spheroidization processing route provides a method for producing microspheres with high uniformity and size control. These factors make the method promising for biomedical, environmental remediation, and energy device applications.pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0003-1561-6994pt_BR
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Física, Grupo de Transiciones de Fase y Materiales Funcionales (GTFMF)-
dc.contributor.affiliationUniversity of Brasilia, Faculty Gama-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Física, Grupo de Películas Delgadas (GPD)-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Química, Grupo de Investigación en Síntesis Organometálica y Catálisis (GISIOMCA)-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Física, Grupo de Transiciones de Fase y Materiales Funcionales (GTFMF)-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Física, Grupo de Transiciones de Fase y Materiales Funcionales (GTFMF)-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Física, Grupo de Transiciones de Fase y Materiales Funcionales (GTFMF)-
dc.contributor.affiliationAcademic Centre for Materials and Nanotechnology, AGH University of Krakow, al. Mickiewicza-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Departamento de Física, Grupo de Transiciones de Fase y Materiales Funcionales (GTFMF)-
dc.contributor.affiliationUniversidad del Valle, Cali, Colombia, Centro de Excelencia en Nuevos Materiales (CENM)-
dc.description.unidadeFaculdade de Ciências e Tecnologias em Engenharia (FCTE) – Campus UnB Gama-
dc.description.unidadeCurso de Engenharia Eletrônica (FCTE-Engenharia Eletrônica)-
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